期刊
CARBOHYDRATE RESEARCH
卷 350, 期 -, 页码 6-13出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2011.12.024
关键词
D-Glucaric acid; Nitric acid oxidation; Diffusion dialysis; Nanofiltration; Ion chromatography; Monopotassium D-glucarate
资金
- USDA Cooperative State Research, Education and Extension Service [2001-34463-10521]
- EPSCoR Lab
The nitric acid oxidation of D-glucose was reinvestigated in an effort to better understand and improve the oxidation and subsequent work up steps. The oxidation was carried out using a computer controlled reactor employing a closed reaction flask under an atmosphere of oxygen which allowed for a catalytic oxidation process with oxygen as the terminal oxidant. Removal of nitric acid from product included the use of both diffusion dialysis and nanofiltration methodologies. Product analysis protocols were developed using ion chromatography. (C) 2012 Elsevier Ltd. All rights reserved.
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