期刊
CARBOHYDRATE RESEARCH
卷 346, 期 12, 页码 1454-1466出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2011.03.036
关键词
Mucin O-glycan core structures; Oxazolidinone protected glycosyl donors; Oligosaccharide synthesis
资金
- Science Foundation Ireland [08/SRC/B1393]
- Science Foundation Ireland (SFI) [08/SRC/B1393] Funding Source: Science Foundation Ireland (SFI)
For the investigation of glycosidases, and for the construction of glycan arrays the p-nitrophenyl- and p-aminophenyl glycosides of mucin O-glycan core structures 1-7 and the 2,6-ST-antigen have been chemically synthesized using D-galactose as a precursor for GalNAc residues. GlcNAc residues have partly been introduced using a 4,6-di-O-benzoyl-2,3-N,O-oxazolidinone-protected donor, which allowed deprotection of the formed di- and tri-saccharides in one step using sodium methoxide. (C) 2011 Elsevier Ltd. All rights reserved.
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