1-Ethyl-3-methylimidazolium-based ionic liquids, [emim] OTf, OTf = trifluoromethanesulfonate (mp = -25.7 degrees C), and [emim] NTf2, NTf2 = bis( trifluoromethanesulfonyl) amide (mp = -25.7 degrees C), have been crystallized by in situ cryocrystallization using a zone-melting technique and found to pack via interionic C-H center dot center dot center dot O and F center dot center dot center dot F interactions.
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