期刊
SOLVENT EXTRACTION AND ION EXCHANGE
卷 24, 期 6, 页码 931-942出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/07366290600952733
关键词
palladium; platinum; gold; Oasis MAX; auto catalysts
This paper presents a new, simple, and rapid procedure for the separation and preconcentration of Au, Pt, Pd, and Rh based on the adsorption of the metals on a commercial solid-phase extraction (SPE) cartridge, Oasis MAX, which contains a polymeric resin with quaternary ammonium substituents. Adsorption studies revealed that the metal affinity towards the adsorbent ranked according to Au >> Pd > Pt whereas Rh was not retained. The elution of the metals was accomplished by using 0.5 M thiourea in 1 M HCl solution. This sorbent effectively recovered Pd and Pt from a spent car catalyst sample containing large amounts of metals such as Al, Fe, and Ce.
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