期刊
SYNTHETIC COMMUNICATIONS
卷 36, 期 15, 页码 2151-2156出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910600636683
关键词
bifenazate; diisopropyl azodicarboxylate; fluoroalcohols; 4-methoxybiphenyl; nitromethane
The synthesis of bifenazate using a two-step procedure has been accomplished with an overall yield of 26%. The procedure involved the Lewis acid-catalyzed electrophilic aromatic substitution of 4-methoxybiphenyl with diisopropyl azodicarcoxylate (DIAD) to give a hydrazinedicarboxylate intermediate that was then subjected to a decarboxylation reaction to give bifenazate.
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