期刊
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
卷 26, 期 16, 页码 3711-3716出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2005.11.013
关键词
milling; niobates; mechanochemical synthesis
We have evaluated the use of a milling map in the mechanochemical synthesis of ceramic oxides. In order to do this we constructed a milling map for NaNbO3, mechanochemically synthesized from a powder mixture of Na2CO3 and Nb2O5. Based on the milling map, we determined the critical or minimum cumulative kinetic energy for the formation of NaNbO3. In addition, we made a comparison between several oxide systems by constructing the milling map on the basis of the experimental data found in the literature. It is shown that a milling map is essential for a comparison of the results of mechanochemical synthesis when different planetary mills and milling conditions are used. (c) 2005 Elsevier Ltd. All rights reserved.
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