期刊
ANALYTICAL METHODS
卷 7, 期 19, 页码 8366-8372出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c5ay01710f
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资金
- National Science Fund of China [21275116]
- Specialized Research Fund for the Doctoral Program of Higher Education [20126101120023]
- Natural Science Foundation of the Shaanxi Province in China [2012JM2013, 2013JM2006]
- Shaanxi Province Educational Committee of China [12JK0576]
- Scientific Research Foundation of the Shaanxi Provincial Key Laboratory [11JS080, 12JS087, 13JS097, 13JS098]
A new sandwich structure nanocomposite of Pt nanoparticles supported on PANI modified graphene was synthesized and used for fabricating a nitrite sensor. The morphology and composition of the nanocomposites were characterized using transmission electron microscopy and X-ray diffraction. Electrochemical investigations indicated that the nanocomposites possess an excellent electrochemical oxidation ability towards nitrites. The sensor exhibited two linear ranges: one from 0.4 mu M to 0.99 mM with a correlation coefficient of 0.9974 and a sensitivity of 485.5 mu A mM(-1) cm(-2); and another from 0.99 mM to 7.01 mM with a correlation coefficient of 0.9981 and a sensitivity of 154.3 mu A mM(-1) cm(-2). The limit of detection (LOD) of this sensing system was 0.13 mu M at a signal-to-noise ratio of 3. Additionally, the sensor exhibited good reproducibility, long-term stability, and anti-interference performance.
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