期刊
SYNTHETIC COMMUNICATIONS
卷 37, 期 22-24, 页码 4105-4109出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910701572753
关键词
deoxygenation; heterogenization; silica-PSCl3; sulfides; sulfoxides
A new solid supported reagent, silica-PSCl3, has been developed for deoxygenation of sulfoxides. With this reagent, conversion of sulfoxides to sulfides occurred cleanly and efficiently at room temperature. Facile isolation of the product was achieved by simple filtration of the by-products without any extensive workup.
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