期刊
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE
卷 633, 期 2, 页码 280-284出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/zaac.200600277
关键词
tetracyanoborate; potassium; vibrational spectroscopy; crystal structure; acetonitrile adduct
The new tetracyanoborate K[B(CN)(4)](CH3CN)-C-. was synthesized by dissolution of the solvent-free K[B(CN)(4)] in acetonitrile and subsequent careful crystallization. The crystal structure has been determined by single-crystal X-ray diffraction. It crystallizes in the orthorhombic space group P2(1)2(1)2(1) with Z = 4. Some comparisons with related structures are made, and the vibrational spectrum is discussed.
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