期刊
ANALYTICAL METHODS
卷 7, 期 6, 页码 2762-2769出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ay02990a
关键词
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资金
- National Natural Science Foundation of China [31171698, 31471643]
- Innovation Research Program of the Department of Education of Hebei for Hebei Provincial Universities [LJRC009]
- Natural Science Foundations of Hebei [B2012204028]
- Scientific and Technological Research Foundation of the Department of Education of Hebei Province [ZD20131033]
Magnetic ordered porous carbon (MOPC-ZSM-5) was synthesized using zeolite ZSM-5 as a template and sucrose as a carbon source. It was used as a magnetic solid-phase extraction adsorbent for the extraction of four neonicotinoid insecticides (acetamiprid, imidacloprid, thiacloprid and thiamethoxam) from river water and peanut milk samples prior to high performance liquid chromatography-ultraviolet detection. The calibration curves for the four neonicotinoid insecticides in the water samples showed linearity from 1.0 to 200.0 ng mL (1) for thiamethoxam, imidacloprid, thiacloprid and 0.5 to 200.0 ng mL (1) for acetamiprid. For the peanut milk samples, the linearity was observed in the range of 6.0-1000.0 ng mL (1) for thiamethoxam, imidacloprid, thiacloprid, and 3.0-1000.0 ng mL(-1) for acetamiprid, respectively. The developed method has been successfully applied for the determination of the four neonicotinoid insecticides in river water and peanut milk samples, and a satisfactory result was obtained.
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