期刊
ARKIVOC
卷 -, 期 -, 页码 34-41出版社
ARKAT USA INC
DOI: 10.3998/ark.5550190.0009.f04
关键词
Dihydropyrimidinone; acylal; solvent-free; Biginelli reaction; heteropoly acid; zinc chloride
资金
- Faculty of Research of Shahid Bahonar University
A novel version of the Biginelli reaction using an acylal as a masked carbonyl functionality together with ethyl acetoacetate and urea or thiourea to give dihydropyrimidinones is reported. The reaction is catalyzed by 12-tungstophosphoric acid (PW), 12-molybdophosphoric acid (PMo) or zinc chloride and performed in one-pot under solvent-free conditions.
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