期刊
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
卷 82, 期 9, 页码 1175-1181出版社
CHEMICAL SOC JAPAN
DOI: 10.1246/bcsj.82.1175
关键词
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资金
- DST [SR/S1/OC-13/2005]
- CSIR [01(1913)/04/EMR-II]
- Government of India
A series of diversely 2-(substituted amino)pyrimidines (along with ring substitution) has been synthesized under solvent- and catalyst-free microwave conditions from substituted guanidines and beta-diketones. The substituted guanidines are synthesized from (S)-methylisothiourea Sulfate and different at-nines (various alkyl, aryl, or heterocyclic and also chiral amines) under microwave irradiation. These two-step reactions are performed in one-pot without isolating any intermediate. This protocol has been successfully applied for the synthesis of bisaminopyrimidines and 2-substituted aminopyrimidines containing chiral moiety where chirality remains undisturbed.
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