期刊
BULLETIN OF MATERIALS SCIENCE
卷 31, 期 6, 页码 885-890出版社
INDIAN ACAD SCIENCES
DOI: 10.1007/s12034-008-0141-y
关键词
Ceramics; chemical synthesis; X-ray microscopy; optical properties; magnetic properties
A solid-state metathesis approach initiated by microwave energy has been successfully applied for the synthesis of orthovanadates, M3V2O8 (M = Ca, Sr, and Ba). The structural, vibrational, thermal, optical and chemical properties of synthesized powders are determined by powder X-ray diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry, magnetic property measurements and diffused reflectance spectra in the UV-VIS range. The direct bandgap of the synthesized materials was found to be 3 center dot 55 +/- 0 center dot 2 eV, 3 center dot 75 +/- 0 center dot 2 eV and 3 center dot 57 +/- 0 center dot 2 eV for Ca3V2O8, Sr3V2O8 and Ba3V2O8, respectively.
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