期刊
ACS OMEGA
卷 3, 期 6, 页码 7124-7132出版社
AMER CHEMICAL SOC
DOI: 10.1021/acsomega.8b00001
关键词
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资金
- Darbari Seth Endowment
- R.T. Mody Distinguished Professor Endowment
- J.C. Bose National Fellowship
- CSIR-NMTLI
- World-Bank's TEQIP Program
- DST-Govt. of India
1-Phenylethanol (PhE) is widely employed in the pharmaceutical industry as an anti-inflammatory and analgesic drug, as well as in chewing gums and yogurts as a food additive. In this work, we have investigated the selective synthesis of 1-phenylethanol (PhE) by hydrogenation of acetophenone using supercritical CO2 as a solvent. Supercritical carbon dioxide (scCO(2)) replaces organic solvent because it is inexpensive, nontoxic, nonflammable, inert, and environmentally benign. Polyurea-based encapsulated mono-and bimetallic catalysts were synthesized and characterized using different characterization techniques. The effects of various reaction parameters, such as co-solvent, catalyst loading, hydrogen pressure, total scCO(2) pressure, and temperature, were studied to determine the reaction kinetics.
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