4.5 Article

Introducing Undergraduates to Research Using a Suzuki-Miyaura Cross-Coupling Organic Chemistry Miniproject

期刊

JOURNAL OF CHEMICAL EDUCATION
卷 92, 期 7, 页码 1217-1220

出版社

AMER CHEMICAL SOC
DOI: 10.1021/ed500551d

关键词

Upper-Division Undergraduate; Laboratory Instruction; Organic Chemistry; Inquiry-Based/Discovery Learning; Catalysis; Chromatography; Grignard Reagents; Organometallics; Synthesis

资金

  1. CNPq
  2. FAPERGS (Brazil)

向作者/读者索取更多资源

A five-week miniproject is described for an upper-division experimental organic chemistry course. The activities include synthesis of a phenylboronic acid via a Grignard reaction and its use in a Suzuki-Miyaura cross-coupling reaction. Technical skills and concepts normally presented in practical organic chemistry courses are covered, including the use of an inert atmosphere (Schlenk tube technique), separation of mixtures (filtration), melting range determination, infrared (IR) spectrum, stoichiometric calculations and gas chromatography techniques.

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