期刊
JOURNAL OF MATERIALS CHEMISTRY
卷 10, 期 5, 页码 1251-1254出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/a908795h
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A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were prepared from BaCl2 hydrate, Pb(Ac)(2), Ti(OPri)(4) and ZrOCl2. All reactions were performed in ethylene glycol, which acted as both a solvent and a growth regulating agent, under atmospheric pressure in a microwave reactor. The products that were obtained were analyzed by using XRD, TEM, XPS, EDX and FT-IR.
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