4.4 Article

Stereoselective electrochemical transformation of alkylidenecyanoacetates and malonate into (E)-3-substituted-2-cyanocyclopropane-1,1,2-tricarboxylates

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TETRAHEDRON LETTERS
卷 41, 期 25, 页码 4937-4941

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(00)00733-4

关键词

electrochemical reactions; stereoselectivity; catalysis; cyclopropanes

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Electrolysis of malonate and alkylidenecyanoacetates in alcohols in the presence of sodium bromide in an undivided cell results in the stereoselective formation of (E)-3-substituted 2-cyanocyclopropane-1,1,2-tricarboxylates in 75-85% yields. (C) 2000 Elsevier Science Ltd. All rights reserved.

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