期刊
TETRAHEDRON-ASYMMETRY
卷 11, 期 12, 页码 2463-2469出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0957-4166(00)00217-2
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The H-1 NMR study of a CD mono-functionalized at its secondary face is presented. It is shown that mono-(3-Tyr-3-deoxy-altro)-beta-CD undergoes a solvent-dependent conformational change. Passing from organic medium to water, a stable self-inclusion complex is formed. Such a folding is accompanied by a local structural modification of the substituted altrose ring, which can be easily detected from the important variation of its H1-H2 coupling constant. (C) 2000 Elsevier Science Ltd. All rights reserved.
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