期刊
TETRAHEDRON LETTERS
卷 41, 期 31, 页码 5873-5876出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(00)00880-7
关键词
electrochemistry; oxidation; alcohols; fluorine and compounds
Electrochemical oxidation of 2,2,2-trifluoroethanol (1) gave trifluoroacetaldehyde 2,2,2-trifluoroethyl hemiacetal (2b), which was more reactive than commercially available trifluoroacetaldehyde ethyl hemiacetal (2a). The high reactivity of 2b was utilized, for example, for the facile synthesis of 1-furyl-2,2,2-trifluoroethanol (4) from furan. (C) 2000 Elsevier Science Ltd. All rights reserved.
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