期刊
JOURNAL OF ORGANOMETALLIC CHEMISTRY
卷 614, 期 -, 页码 70-73出版社
ELSEVIER SCIENCE SA
DOI: 10.1016/S0022-328X(00)00631-8
关键词
arsenic; cage compounds; magnesium; metalations; tin
The magnesiation of H2AsSi'Pr-3 yields the tetramer [(THF)MgAsSi'Pr-3](4) (1) with a central Mg4As4 heterocubane moiety. The reaction of Sn[N(SiMe3)(2)](2) with triisopropylsilylarsane gives the hexamer [(SnAsSiPr3)-Pr-i](6) (2) with an inner hexagonal Sn,As, prism. The molecular structures of both these compounds have been determined. (C) 2000 Elsevier Science B.V. All rights reserved.
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