期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 123, 期 2, 页码 199-202出版社
AMER CHEMICAL SOC
DOI: 10.1021/ja003104i
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资金
- NCRR NIH HHS [RR02002] Funding Source: Medline
- NIGMS NIH HHS [R01 GM039764] Funding Source: Medline
One- and two-dimensional Li-6 and N-15 NMR spectroscopic studies of lithium diisopropylamide (LDA) solvated by substoichiometric concentrations of oxetane, THF, Et2O, and diisopropylamine are described. Partially solvated dimers and trimers are identified. Possible benefits of carrying out organolithium chemistry at low ligand concentrations are discussed.
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