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High-yielding TfOH-catalyzed condensation of phenols with aromatic aldehydes at high pressure. A model synthesis of the benzylidene biphenol key skeleton of blepharismins

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TETRAHEDRON LETTERS
卷 42, 期 13, 页码 2493-2496

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)00208-8

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An approach to the benzylidene biphenol key component of blepharismins, photoreceptor pigments isolated from Blepharisma japonicum, is reported. This method relies on an efficient TfOH-catalyzed condensation of phenols with aromatic aldehydes in EtOH as a solvent at 3 kbar pressure. (C) 2001 Elsevier Science Ltd. All rights reserved.

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