期刊
NEW JOURNAL OF CHEMISTRY
卷 25, 期 4, 页码 528-530出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b009556g
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The reaction of Al2Cl6 with an excess of Ph2Si(OH)(2) in THF in the presence of pyridine yielded new anionic and cyclic aluminosiloxanes: the structure of the anionic complex is composed of separated pyridinium cations and aluminosiloxane anions dth a tetrahedral arrangement around the Al atom, which is similar to that in natural aluminosilicates; the core of the cyclic aluminosiloxane is a twelve-membered Al2Si4O6 ring in a chair conformation, which contains a Cl group on each of the two Al atoms.
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