期刊
ORGANIC LETTERS
卷 3, 期 8, 页码 1129-1131出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol015577f
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资金
- NIGMS NIH HHS [GM 46059] Funding Source: Medline
Enantiomerically enriched 2,3 disubstituted cyclopentanones were prepared via copper-catalyzed 1,4-reduction of 3-substituted cyclopentenones followed by alkylation of the resulting silyl enol ether. Using this procedure, trans-2,3-disubstituted cyclopentanones were produced in moderate to good overall yields (42-67%) and with excellent enantiomeric and diastereomeric excesses. The reduction and alkylation were performed in a single reaction vessel.
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