期刊
TETRAHEDRON LETTERS
卷 42, 期 22, 页码 3701-3703出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(01)00549-4
关键词
alkyne metathesis; microwave; silanol
The catalytic mixture based on Mo(CO), was re-examined in the metathesis of 4-methoxytolan. Silanols (4) or (5) were found to be very active as co-catalysts. The metathesis of functional alkynes was convenient and rapidly achieved in octane as solvent under microwave irradiation in a resonance cavity. (C) 2001 Elsevier Science Ltd. All rights reserved.
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