期刊
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
卷 57, 期 -, 页码 m298-m300出版社
MUNKSGAARD INT PUBL LTD
DOI: 10.1107/S1600536801009667
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The crystal structure of tetra-mu (3) -tert-butoxo-tetrakis(methylzinc) tetrahydrofuran (THF) solvate, [Zn-4(CH3)(4)(C4H9O)(4)].C4H8O, has been determined at 230 (1) K. The structure is based on a ((BuOZnMe)-Bu-t)(4) pseudo-cube and contains one lattice molecule of tetrahydrofuran per ((BuOZnMe)-Bu-t)(4) unit. Comparison with a previously reported unsolvated structure of methylzinc tert-butoxide suggests that this also contains lattice THF.
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