期刊
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
卷 8, 期 -, 页码 300-307出版社
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.8.32
关键词
asymmetric reduction; binolphosphoric acid; Bronsted acid; Hantzsch dihydropyridine; IR spectroscopy; real-time analysis
资金
- Excellence Initiative of the German federal government
- European Research Council
- Excellence Initiative of the German state government
The asymmetric organocatalytic hydrogenation of benzoxazines, quinolines, quinoxalines and 3H-indoles in continuous-flow microreactors has been developed. Reaction monitoring was achieved by using an inline ReactIR flow cell, which allows fast and convenient optimization of reaction parameters. The reductions proceeded well, and the desired products were isolated in high yields and with excellent enantioselectivities.
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