期刊
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
卷 7, 期 -, 页码 1124-1129出版社
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.7.129
关键词
azepinones; azides; continuous flow; nitrenes; photochemistry
资金
- Max Planck Society
- AstraZeneca RD
- Macclesfield, UK
- Fonds de Recherche sur la Nature et les Technologies, Quebec
Photolysis of aryl azides to give nitrenes, and their subsequent rearrangement in the presence of water to give 3H-azepinones, is performed in continuous flow in a photoreactor constructed of fluorinated ethylene polymer (FEP) tubing. Fine tuning of the reaction conditions using the flow reactor allowed minimization of secondary photochemical reactions.
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