期刊
BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY
卷 5, 期 -, 页码 -出版社
BEILSTEIN-INSTITUT
DOI: 10.3762/bjoc.5.34
关键词
continuous flow system; microreactor; radical carbonylation; radical mediator; V-65
资金
- JSPS/MEXT Japan and MCPT/NEDO
Radical-based carbonylation reactions of alkyl halides were conducted in a microflow reactor under pressurized carbon monoxide gas. Good to excellent yields of carbonylated products were obtained via radical formylation, carbonylative cyclization and three-component coupling reactions, using tributyltin hydride or TTMSS as a radical mediator.
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