期刊
RUBBER CHEMISTRY AND TECHNOLOGY
卷 74, 期 5, 页码 803-813出版社
AMER CHEMICAL SOC INC
DOI: 10.5254/1.3547654
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There is increased technological interest to use blends of various dissimilar elastomers in applications for which service, material availability, or cost of a single elastomer do not provide the necessary processing, vulcanizate, or economic properties. Properties of polyblends are sensitive to variations in the amounts of the individual polymers used. Therefore, there is a need for developing a variety of analytical tools that will enable the compounder to monitor the consistency of blend compositions. In this study, the feasibility of using pyrolysis-GC/MS and thermogravimetric analysis (TGA) to estimate the blend composition of SBR/NBR blends was investigated. Pyrolysis-GC/MS degradation products that are characteristic of each polymer were identified. The GC/MS peak areas were used to determine the blend composition. The blend compositions were estimated by TGA from the linear correlation between the polymer composition and the temperature required to pyrolyze a sample to a specific % weight loss. The results obtained by pyrolysis-GC/MS and TGA were compared to calculated blend ratios of SBR/NBR in order to estimate the accuracy of the test methods presented in this study.
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