期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 1, 页码 22-26出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo0057351
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The synthesis of a series of enantiopure malonaldehyde monocycloacetals is described. Treatment of 8b with L-tryptophan methyl ester, 5-methoxytryptamine, and tryptamine, respectively, in the Pictet-Spengler condensation gave the corresponding enantiomerically pure key precursors 1-3 and 17-21 in only two steps. Using a chiral amino-diol successfully realized the kinetic resolution of racemic carbolines 23 and 24.
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