期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 4, 页码 1045-1056出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo010270f
关键词
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The reduction of N-protected amino ketones can be carried stereoselectively to produce either the syn- or anti-amino alcohol diastereomer. Carbamate-protected amino ketones can be reduced predictably and selectively to anti-amino alcohols with LiAlH(O-t-BU)(3) in ethanol at -78 degreesC. N-Trityl-protected amino ketones can be reduced selectively to syn-amino alcohols with LiAlH(O-t-Bu)(3) in THF at -5 degreesC.
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