期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 10, 页码 3502-3505出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo011057m
关键词
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A series of molecules of therapeutic interest, possessing the new skeleton of 1-H-benzo [c] pyrido [2,3,4-kl]-acridine with acyl or aminoacyl and methoxy or aminoalkoxy substituents on the aromatic homocycles were synthesized by means of a Friedlander-type reaction. The requisite 5-aminodihydroquinoline-4-ones 1, whose preparation is described, were reacted with the appropriate alpha-tetralones 2 using an acidic catalyst (PPTS) under azeotropic conditions. Optimized reaction time and yield depend on temperature, which must not be below 90 degreesC.
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