期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 11, 页码 3861-3865出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo0255936
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资金
- NIGMS NIH HHS [GM 35249] Funding Source: Medline
Samarium(II) iodide, in the presence of catalytic amounts of nickel(II) iodide, has been used to promote intramolecular conjugate additions of alkyl halides onto alpha,beta-unsaturated lactones. This process has been shown to be applicable to a number of alpha,beta-unsaturated lactones, including tetrasubstituted olefins, and has been demonstrated to be quite general for the formation of saturated bicyclic and tricyclic lactones. The method presented herein provides a mild, efficient process to form structurally complex lactones from simple precursors.
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