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Polymer-supported reagents for methylphosphorylation and phosphorylation of carbohydrates

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BIOORGANIC & MEDICINAL CHEMISTRY LETTERS
卷 12, 期 14, 页码 1863-1866

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PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0960-894X(02)00266-4

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Two polymer-supported reagents for methylphosphorylation and phosphorylation of carbohydrates have been developed. p-Hydroxybenzyl alcohol and beta-mercaptoethanol were immobilized on cross-linked divinylbenzene-polystyrene copolymer and conjugated with methyl N,N-diissopropylchlorophosphoramidite. Carbohydrates were reacted with polymer-bound phosphitylating reagents. Further oxidation, with or without the methoxy group deprotection, and cleavage yielded methylphosphorylated or phosphorylated carbohydrates, respectively. (C) 2002 Elsevier Science Ltd. All rights reserved.

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