期刊
THERMOCHIMICA ACTA
卷 391, 期 1-2, 页码 119-127出版社
ELSEVIER
DOI: 10.1016/S0040-6031(02)00169-7
关键词
DSC; TGA; kinetics; model-free analysis; model-fit; non-linear regression
Model-free kinetic analysis is a powerful tool to estimate the activation energy of processes, investigated by various isothermal or dynamic measurements. On the basis of real measurements and simulations we demonstrate that limitations of application exist. Conditions are listed under which estimated values of activation energy could be incorrect. (C) 2002 Elsevier Science B.V. All rights reserved.
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