期刊
ORGANIC LETTERS
卷 4, 期 18, 页码 3087-3089出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol026382q
关键词
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资金
- NIGMS NIH HHS [GM 62120, R01 GM062120, R01 GM062120-05] Funding Source: Medline
[GRAPHICS] A highly convergent synthesis of the angiogenesis inhibitor luminacin D has been achieved in 13 linear steps (19 steps total, 5.3% overall yield) utilizing a samarium(II) iodide-mediated mixed tandem aldol/Evans-Tishchenko reaction to construct the carbohydrate precursor. The modular synthetic design will allow derivatization at key positions necessary for biochemical mode of action studies.
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