期刊
TETRAHEDRON LETTERS
卷 43, 期 37, 页码 6629-6631出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(02)01453-3
关键词
amines; reductive cyclization; hydriodic acid; pyrrolobenzodiazepines
The reduction of aromatic azido compounds to the corresponding amines with hydriodic acid has been investigated and found to result in high yields. This reductive methodology which proceeds under non refluxing condition has been extended for the synthesis of DNA-interactive pyrrolo[2,1-c][1,4] benzodiazepine antibiotics. (C) 2002 Elsevier Science Ltd. All rights reserved.
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