期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 19, 页码 6841-6844出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo025745x
关键词
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Bulky trialkylsilyl-protected alkynes such as triethylsilyl (TES), tert-butyldimethylsilyl (TBS), and tri-isopropylsilyl (TIPS) acetylenes underwent the Cadiot-Chodkiewicz cross-coupling reaction with different bromoalkynes to form a variety of synthetically useful unsymmetrical diynes in good yields. The diyne alcohol 10 was transformed regio- and stereoselectively into enynes by hydrotelluration, carbometalation, and reduction reactions.
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