4.5 Article

High-pressure powder x-ray diffraction experiments on Zn at low temperature

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JOURNAL OF PHYSICS-CONDENSED MATTER
卷 14, 期 44, 页码 10563-10568

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IOP PUBLISHING LTD
DOI: 10.1088/0953-8984/14/44/333

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High-pressure powder x-ray diffraction experiments have been performed on Zn with a He-pressure medium at low temperature. When the sample was compressed in the He medium at low temperature, large nonhydrostaticity developed, yielding erroneous lattice parameters. On the other hand, when the pressure was changed at high temperatures, good hydrostaticity was maintained. No anomaly in the volume dependence of the c/a axial ratio has been found. (Some figures in this article are in colour only in the electronic version).

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