期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 67, 期 26, 页码 9192-9199出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo020501y
关键词
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A highly stereoselective asymmetric synthesis of (-)-sedamine and (-)-lobeline is described from benzaldehyde in 16 and 17 steps with an overall yield of 20% and 14%, respectively. The key intermediate syn-3,4-epoxyalcohol was prepared in a highly diastereomeric fashion (>99% ee, dr) and served as a common intermediate for both alkaloids.
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