期刊
ORGANIC LETTERS
卷 5, 期 5, 页码 765-768出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol034042e
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资金
- NIGMS NIH HHS [GM-50151] Funding Source: Medline
[GRAPHICS] The antitumor antibiotic phloeodictine All (2) has been synthesized by a convergent seven-step route in 8% overall yield. The key step was the Eguchi aza-Wittig reaction of 6 to give 13 followed by a retro Diels-Alder reaction to liberate 5. Addition of 11-dodecenylmagnesium bromide to 5 to give 4b, alkylation with 18b, and deprotection completed the first synthesis of 2.
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