期刊
TETRAHEDRON LETTERS
卷 44, 期 13, 页码 2657-2660出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(03)00347-2
关键词
cyclodextrin; hydrosilylation; chiral stationary phases; enantioseparation
A novel cyclodextrin derivative: mono(6(A)-N-allylamino-6(A)-deoxy)perphenylcarbamoylated beta-cyclodextrin was synthesized. Hydrosilylation with (EtO)(3)SiH and then reaction of the reactive siloxane with pristine silica gel afforded a facile entry into a durable, structurally well-defined chiral stationary phase capable of enantioseparation of a variety of racemic drugs. (C) 2003 Elsevier Science Ltd. All rights reserved.
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