期刊
TETRAHEDRON LETTERS
卷 44, 期 15, 页码 3093-3096出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(03)00550-1
关键词
trienylboronic acid; Suzuki coupling; conjugated pentaene; 11Z-retinal; iododiene
Trienylboronic acid 1a was prepared from iodotriene 3, which was coupled with (2Z,4Z)-3-aryl-5-iodo-2,4-pentadienol 9 by Suzuki coupling reaction to give geometrically pure 13-aryl substituted (11Z)-retinol 10. Oxidation of 10 gave 13-aryl substituted (11Z)-retinal 11. (C) 2003 Elsevier Science Ltd. All rights reserved.
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