期刊
BIOCHEMICAL SYSTEMATICS AND ECOLOGY
卷 31, 期 5, 页码 477-485出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0305-1978(02)00177-1
关键词
Onosma arenaria; Boraginaceae; pyrrolizidine alkaloids; uplandicine; NMR; gas liquid chromatography (GLC); GLC-mass spectrometry
Uplandicine, a 1,2-unsaturated pyrrolizidine alkaloid esterified with acetyl and echimidinyl moieties at C-7 and C-9, respectively, was isolated as a major component from the alkaloid extract of Onosma arenaria. Its structure was confirmed by MS (EI and positive FAB), 1H- and 13C-NMR analysis. Furthermore, nine minor alkaloids were identified on the basis of mass spectral data and/or Kovats retention indices. (C) 2003 Published by Elsevier Science Ltd.
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