期刊
TETRAHEDRON LETTERS
卷 44, 期 26, 页码 4915-4917出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(03)01126-2
关键词
alkylbenzene; selective oxidation; molybdenum peroxo complex; hydrogen peroxide
The molybdenum(VI) peroxo complex 1, synthesized from the reaction of MoO2 with H2O2 and 3,5-dimethylpyrazole (dmpz), selectively oxidizes benzylic C-H bonds of alkylbenzenes to the corresponding alcohols and ketones in moderate to good yields in the presence of H2O2 in acetonitrile under reflux (ca. 80degreesC). (C) 2003 Elsevier Science Ltd. All rights reserved.
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