期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 68, 期 13, 页码 5193-5197出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo034369t
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A nonphotochemical synthetic route to 3-hexahelicenol is reported. It involves a key [2+2+2] cycloisomerization of CH3O-substituted triyne that is readily available from 1-methoxy-3-methylbenzene and 1-bromo-2-(bromomethyl)naphthalene. Further functional group transformations led to 3-CO2CH3, 3-NH2, 3-PPh2, and 3-SC(O)N(CH3)(2) substituted hexahelicenes.
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