期刊
JOURNAL OF ORGANIC CHEMISTRY
卷 68, 期 14, 页码 5439-5444出版社
AMER CHEMICAL SOC
DOI: 10.1021/jo026753g
关键词
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Carbonate anions resulting from reaction of primary or secondary alcohols with carbon dioxide, when added to methanesulfonic anhydride in cooled acetonitrile solution, yield methanesulfonyl carbonates, a new class of synthetic intermediate. Base-mediated reaction of the methanesulfonyl carbonates with alcohols, thiols, and amines yields carbonates, thiocarbonates, and carbamates, respectively. Overall yields for the three steps vary from 19% to 42%.
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