期刊
TETRAHEDRON LETTERS
卷 44, 期 32, 页码 6007-6009出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/S0040-4039(03)01473-4
关键词
benzo[b]thiophenes; borylation; palladium; Suzuki coupling; dehydroamino acids
Several benzo[b]thienyidehydroamino acids were prepared by one-pot palladium-catalyzed borylation and Suzuki coupling (BSC) from bromobenzo[b]thiophenes containing EDG (OMe or Me), as the component to be borylated with pinacolborane, and pure stereoisomers of beta-bromodehydroamino acid derivatives. To our knowledge it is the first time that the BSC reaction involves a non aromatic system. (C) 2003 Elsevier Ltd. All rights reserved.
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