期刊
ORGANIC LETTERS
卷 5, 期 21, 页码 3883-3885出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol035438t
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资金
- NIGMS NIH HHS [R01 GM058877, GM58877, R01 GM054623-08] Funding Source: Medline
[GRAPHICS] The stereoselective intramolecular reductive etherification of delta-trialkylsilyloxy substituted ketones with catalytic bismuth tribromide and triethylsilane provides a convenient method for the construction of cis-2,6-disubstituted tetrahydropyrans. This method was highlighted in the key step of an expeditious total synthesis of the antibiotic, (-)-centrolobine.
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